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2,2,6,6-tetramethylpiperidine


tetramethylpiperidine TMP
Chemical name 2,2,6,6-tetramethylpiperidine
Chemical formula C9H9N
Molecular mass 141.25 g/mol
Melting point 42 °C
Boiling point 152 °C
Density 0.83 g/cm3
CAS number 768–66–1
SMILES
Disclaimer and references

2,2,6,6-tetramethylpiperidine or TMP or HTMP is a clear light yellow liquid with an amine odor. This amine is used in chemistry as a base because it can dissolve in organic solvents unlike ordinary bases like potassium hydroxide. There are many ways to synthesise TMP. One recent method [1] starts with a conjugate addition reaction of ammonia to phorone. The intermediate triacetone amine is then reduced in a Wolff-Kishner reaction.



TMP is the starting material for an even stronger base Lithium tetramethylpiperidide and the radical species TEMPO


External links

References

  • [1] A Large-Scale Low-Cost Access to the Lithium 2,2,6,6-Tetramethylpiperidide Precursor Detlef Kampmann, Georg Stuhlmüller, Roger Simon, Fabrice Cottet, Frédéric Leroux, Manfred Schlosser Synthesis 2005 1028–1029 Abstract







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